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Do you connect it direct to the MAC or via a hub? Try direct if via a hub.
Also, Calibre now mounts and unmounts the Cybook correctly so try using that and see if it helps.
On my Mac Mini I can happily connect nad eject without any issues now although I did have issues early on with the the last release of teh Cybook firmware, but these dissappeared with firmware 796 but that could just be coincidence.
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